Non-destructive observation of internal fatigue crack growth in Ti–6Al–4V by using synchrotron radiation μCT imaging

Significance Statement

Fumiyoshi Yoshinaka and colleagues carried out a research to reveal the propagation process of internal crack growth in titanium alloys Ti-6Al-4V. The research published in International Journal of Fatigue investigated the very high cycle fatigue properties of titanium alloys.

The study used synchrotron radiation micro computed tomography μCT technique to observe internal fatigue crack growth which is small to be detected by commonly used X-ray CT. The synchrotron radiation facility is located in Hyogo, Japan. With this facility, high brightness synchrotron radiation of one million time can be achieved. Super Photon ring-8GeV (SPring-8) is one of the world largest third-generation synchrotron radiation facilities.

The research team explained that fatigue test was carried out using a high response and transportable axial hydraulic servo fatigue testing machine that was developed in the laboratory. The imaging system consists of light source, optical system, a detector, and a specimen. In Ti–6Al–4V, the size of the initial crack would be a few tens of micrometers. Nakamura and his co-researcher assumed fatigue cracks close under unloading conditions. It seems to be difficult to detect such a closed small crack, so a tensile loading grip was developed to open the crack during μCT imaging.

To find an internal small crack, the projected image perpendicular to the loading axis was carefully examined in the parallel part of the pre-fatigued specimen. As a result, a circular dark region was observed in the images of the first μCT imaging.

The propagation of an internal fatigue crack in Ti–6Al–4V was non-destructively observed by synchrotron radiation μCT imaging to clarify the crack growth rate in very high cycle fatigue. The results show that the internal crack propagated quite slowly at a rate of less than 10-10 m/cycle.

The shape and dimension of the internal fatigue crack observed by μCT imaging matched those measured on the surface profile of the fracture surface obtained by 3D-SEM. The accuracy of μCT imaging was considered sufficient to give a reliable image of the internal crack propagation. The rate of the internal crack was similar to that of the surface crack in high vacuum which was obtained by their previous research, but was significantly lower than that in air.

These findings suggest that the reason for the great difference between the propagation rates of internal and surface cracks is the difference in environments around them.

Non-destructive observation of internal fatigue crack growth in Ti–6Al–4V by using synchrotron radiation μCT imaging. Advances in EngineeringNon-destructive observation of internal fatigue crack growth in Ti–6Al–4V by using synchrotron radiation μCT imaging. Advances in Engineering

Non-destructive observation of internal fatigue crack growth in Ti–6Al–4V by using synchrotron radiation μCT imaging. Advances in Engineering

 

About the author

Fumiyoshi Yoshinaka is a Ph. D. candidate in engineering at Hokkaido University. He received the B.S. degree from Hokkaido University, Hokkaido, Japan, in 2013 and the M.S. degree from Hokkaido University, Hokkaido Japan, in 2015. His research interest is on the very high cycles fatigue in high strength metallic materials.

His research involves the non-destructive observation of the internal fatigue crack by using high resolution X-ray CT and the fatigue properties in vacuum environments. He is a JSPS Research Fellow since April 2016. 

About the author

Dr. Takashi Nakamura is a professor of the division of Mechanical and Space Engineering at Hokkaido University, Sapporo, Japan. He received his Ph.D. from Tokyo Institute of Technology in 1995 after 4-year work as a research associate at TIT and 5-year development work on motion control machines at Moog Japan Ltd. His current research is focusing on the very high cycle fatigue of high strength materials, fatigue in ultra-high vacuum, and degradation of polymers in space environment. 

About the author

Shinya Nakayama was born in 1988. He received the B.S. degree from Hokkaido University, Hokkaido, Japan, in 2012 and the M. S. degree from Hokkaido University, Hokkaido Japan, in 2014. He currently works at Nippon Steel & Sumitomo Metal Corporation, Japan, as an engineer. 

About the author

Dr. Daiki Shiozawa is an associate professor of Department of Mechanical Engineering at Kobe University, Kobe, Japan. After he received his Ph.D. from Osaka University in 2004, he worked for Kobe University as an assistant professor for 9 years and attained the current position.

His research area is non-destructive evaluation of materials using synchrotron radiation and dissipated energy. 

About the author

Dr. Yoshikazu Nakai is a Professor of Department of Mechanical Engineering at Kobe University, Kobe, Japan. After he received his Ph.D. from Kyoto University, Japan in 1983, he performed postdoctoral research at Lehigh University, Bethlehem, Pennsylvania, USA and Associate Professor of Department of Mechanical Engineering, Osaka University, Suita, Osaka, Japan.

He was vice-president of the Society of Materials Science, Japan, and chairman of International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM’11).  He also served as member of the executive board of Japanese Society of Mechanical Engineers.

Dr. Nakai’s research interest is in the area of fatigue of materials, with an emphasis on micro mechanisms of crack initiation and propagation. 

About the author

Dr. Kentaro Uesugi received the Ph.D. degree from the University of Tokyo, Tokyo, in 2013. He is a researcher of JASRI, is now working as a beamline scientist at synchrotron radiation facility SPring-8 in Japan from 2000. His research interest is development of x-ray micro-tomography system using synchrotron radiation. 

Journal Reference

Fumiyoshi Yoshinaka1, Takashi Nakamura2, Shinya Nakayama1, Daiki Shiozawa3, Yoshikazu Nakai3, Kentaro Uesugi4, Non-destructive observation of internal fatigue crack growth in Ti–6Al–4V by using synchrotron radiation μCT imagingInternational Journal of Fatigue , 2016 , 93 , Part 2 , 397-405.

[expand title=”Show Affiliations”]
  1. Division of Mechanical and Space Engineering, Graduate School of Engineering, Hokkaido University, Kita 13, Nishi 8, Kita-ku, Sapporo, Hokkaido 060–8628, Japan.
  2. Division of Mechanical and Space Engineering, Faculty of Engineering, Hokkaido University, Kita 13, Nishi 8, Kita-ku, Sapporo, Hokkaido 060–8628, Japan.
  3. Department of Mechanical Engineering, Kobe University, 1-1, Rokkodai-cho, Nada-Ku, Kobe 657-8501, Japan.
  4. Japan Synchrotron Radiation Research Institute, 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5198, Japan.
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