Integrated pre-concentrator gas sensor microsystem for ppb level benzene detection

Significance Statement

Researchers led by Professor Andreas Schütze from Saarland University in Germany designed a device capable of detecting ppb levels of volatile organic compounds. The research was in collaboration with the Fraunhofer Institute ICT, specialists in preconcentration methods, and Swiss industrial partner, SGX Sensortech SA, which specializes in air quality sensors and modules. The prototype was tested for its performance using benzene as a testing compound. A video of the technology is found in this link (http://www.sensindoor.eu/film).

To detect such small concentrations of these gases without expensive and time-consuming analytical measurements like GC–MS analysis, solid state gas sensors can be used in combination with a novel pre-concentrator. In this investigation, metal organic framework materials have been characterized regarding their suitability as pre-concentrator materials for benzene, i.e., their adsorption potential at low temperatures and the desorption characteristics at elevated temperature were studied. For comparison, the adsorption potential was also tested for toluene. Metal organic frameworks showed a higher partition coefficient than Tenax®TA, a state-of-the-art commercial adsorbent material.

Schütze emphasizes: “The novel integrated microsystem combines sensitivity and selectivity comparable to analytical methods with the low-cost of sensor technology.” The study is now published in Sensors and Actuators B: Chemical.

The technology developed by the authors accurately and selectively measures hazardous volatile organic compounds and is expected to control and prevent Sick Building Syndrome, a major hazard both in the workplace and in private homes, by demand controlled ventilation.

The authors acknowledge funding received for the project from the European Union’s Seventh Framework Programme for research, technological development and demonstration under grant agreement No 604311, Project SENSIndoor.

 

 Integrated pre-concentrator gas sensor microsystem for ppb level benzene detection.Advances in Engineering

About the author

Martin Leidinger received his diploma in mechatronics engineering from Saarland University, Saarbrücken, Germany, in 2013. He is currently a Ph.D. student at the Lab for Measurement Technology at Saarland University. His main research interests are in the fields of dynamic gas sensor operation, gas pre-concentration and design of gas mixing systems for trace gases. 

About the author

Max Rieger studied chemistry at the University of Würzburg and received his diploma in 2011 in the field of theoretical and physical chemistry. Since 2011 he is part of the analytics and detection group within the department of energetic materials at the Fraunhofer Institute for Chemical Technology in Pfinztal. He is involved in porous materials characterization and preconcentration methods for explosive and hazardous materials. 

About the author

Christine Alépée studied micro-engineering and received her PhD from the Swiss Federal Institute of Technology in Lausanne in 2000. She joined MiCS/SGX in 2001 where she has focused her activities on the development of gas sensing MEMS based on various gas detection principles with the goal of improving commercial gas sensors in terms of sensing properties, power consumption, reliability, and fabrication costs. 

About the author

Tilman Sauerwald received his PhD in 2007 at the University of Giessen working on the influence of surface reactions to the multi-signal generation of metal oxide sensors. Since 2011 he is working at the Lab for Measurement Technology at Saarland University. His current focus is the detection of trace gases by developing model based techniques for multi-signal generation as well as combination with analytical approaches. 

About the author

Andreas Schütze studied Physics and received his doctorate in Applied Physics from Justus-Liebig-Universität in Gießen in 1994 with a thesis on micro gas sensor systems. After some years in industry, he joined the University of Applied Sciences in Krefeld, Germany, as professor for Microsystems Technology from 1998 to 2000.

Since 2000 he is a full professor for measurement science and technology in the Department of Systems Engineering at Saarland University, Saarbrücken, Germany. His research interests include microsensors and microsystems, especially advanced chemical sensor systems, both for gas and liquid phase, for security and control applications. 

Journal Reference

Martin Leidinger1, Max Rieger2,, Tilman Sauerwald1, Christine Alépée3, Andreas Schütze1Integrated pre-concentrator gas sensor microsystem for ppb level benzene detection,  Sensors and Actuators B: Chemical, Volume 236, 2016, Pages 988–996.

[expand title=”Show Affiliations”]
  1. Lab for Measurement Technology, Saarland University, D-66123 Saarbrücken, Germany
  2. Fraunhofer Institute for Chemical Technology ICT, D-76327 Pfinztal, Germany
  3. SGX Sensortech SA, CH-2035 Corcelles-Cormondrèche, Switzerland
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