Balancing Strength and Ductility: The Dual Role of Gradient Structures and Carbides in Fatigue Resistance of High-Strength Steel

Significance 

Fatigue fracture is one of the major challenges in materials engineering, especially when it comes to high-strength steels. These steels play an essential role in bridges, skyscrapers, and transportation systems, where they must endure repeated stress over time. Their ability to resist fatigue failure is vital not just for performance but also for safety. Despite all the advancements in strengthening techniques—like refining grain size, phase transformations, or solid solution hardening—there is still a major challenge which is finding the right balance between making the material strong and in the same time keep it ductile. Most conventional methods tend to lean too far in one direction, often creating brittle materials that can fail catastrophically under repeated stress. Things get even trickier when carbides enter the picture. These tiny particles in steel microstructure are helpful for boosting strength, but they have a downside: they often become starting points for cracks, which can speed up fatigue failure. The size, spread, and how these carbides interact with the surrounding material all have a big say in how the steel handles fatigue. To find a solution, researchers have turned to a newer approach called gradient structures. These are essentially changes in microstructural properties—like grain size or composition—throughout the material. The idea is that these gradients can help spread out stress more evenly, reducing weak spots where cracks could grow. But putting gradient designs into steels that already have carbides is no simple task. Understanding how the two work together under repeated stress requires a deep dive into their combined effects.

New research paper published in Journal of Materials Science and conducted by graduate students Meichen Pan, Li Yang, Dr. Xiaoyu Zheng, Dr. Hong Mao, Associate Professor Yi Kong & led by Professor Yong Du from Central South University examined how gradient high-strength steels with carbides behave under cyclic loading. Most studies so far have looked at carbides and gradient structures separately, leaving a lot of unanswered questions about how they interact. Adding to the difficulty, experimental methods often fall short when it comes to replicating the complexity of gradient structures at the micro-scale. To bridge this gap, the team relied on computational simulations that could lead to better and more durable materials. The researchers used finite element modeling to examine how stress and strain behave in high-strength steel under repeated loading. They also wanted to see how cracks form and spread. To make the simulations realistic, they factored in the Hall–Petch effect, which explains how grain size affects a material’s strength. Their focus was on Q690 steel, a popular choice in engineering projects, and they based its mechanical properties on earlier experimental data. In their experiments, they modeled gradient structures with grain sizes ranging from 5 to 20 micrometers and added carbides—brittle inclusions that mimic real-world material challenges.

To get a closer look at how cracks grow, the team introduced tiny prefabricated microcracks into the simulated material. These were placed in specific areas to help them zero in on crack propagation without spending excessive time on the initial phases. Using a method called Voronoi algorithms, they created two-dimensional models that divided the material into zones with different grain sizes, imitating gradient structures. Carbides were added as small, brittle zones within the steel matrix to study how they influenced stress concentrations and affected the paths cracks took. The authors applied cyclic displacement loads to mimic real-world conditions, with the loading alternating between tension and compression. The results were exciting. Gradient structures helped distribute stress more evenly especially in areas with finer grains which showed higher strength. These fine-grained zones acted like barriers and slowed down the progression of cracks and delayed material failure. On the other hand, coarse-grained regions were less effective at stopping cracks and led to quicker breakdowns. Carbides added another layer of complexity. They concentrated stress around themselves and caused cracks to spread along weaker grain boundaries. Their size and distribution played a major role in how much they shortened the material’s lifespan. One of the standout findings was the push-and-pull relationship between gradient structures and carbides. Gradient structures were great at slowing crack growth and boosting fatigue resistance, but carbides had the opposite effect, speeding up crack initiation and spreading. Fine-grain gradients were better at counteracting these problems than coarse-grain ones. However, the researchers pointed out that even the best gradient design could not completely cancel out the negative impact of carbides. This highlighted the need for a careful balance between the two when designing materials meant to resist fatigue.

To wrap things up, Professor Yong Du and his team have made a real advancement in how we think about designing and improving high-strength steels for use under repeated stress. Their work sheds light on the complicated relationship between gradient structures and carbides during fatigue fracture. At the heart of this research is a solution to a long-standing problem in materials engineering: how to boost both strength and ductility without sacrificing one for the other. The findings highlight how microstructural gradients can help distribute stress more evenly and slow down the spread of cracks. This has huge potential for extending the lifespan of materials used in demanding fields like infrastructure, aerospace, and automotive manufacturing. According to the authors, one of the standout aspects of their study is the discovery that fine-grain gradient structures can make a big difference in fatigue resistance. By creating a more even stress distribution, these gradients act like a shield, blocking cracks before they can grow too much. This is a big improvement over traditional methods that rely on uniform microstructures, which often fall short when dealing with localized stress. On top of that, the researchers’ use of computational modeling offers a practical and cost-effective way to explore complex microstructures. It’s a valuable alternative to experiments, which can be tough to carry out when working with sophisticated designs. What’s particularly exciting about this research is how it bridges theory and real-world application. By including carbides in their fatigue models, the team provided clear, actionable guidelines for designing high-strength steels where carbides are a given. The results suggest that with the right balance—careful control over carbide size and distribution paired with strategic gradient structuring—it’s possible to create steels that stand up better to fatigue. This dual approach could be a game changer for industries where materials face constant stress. Beyond the immediate findings, the study opens the door for more innovation in gradient engineering. It encourages researchers to explore other types of gradients, like those involving composition or phase changes, to tackle similar challenges.

About the author

Yong Du is a full professor at Central South University (CSU) of China. He received his PhD from CSU in 1992. From 1993 to 2003, he continued his research in Tokyo Institute of Technology, University of Barcelona, Clausthal University of Technology, University of Vienna, and University of Wisconsin at Madison. His research fields include thermodynamics, phase diagram, diffusion, microstructure characterization, and structure-property correlation of light alloys, cemented carbides, hard-coating, and nuclear materials. He has published 925 papers in well-known international journals, such as Chem. Mater., Acta Mater., Phys. Rev. B, Scripta Mater., Surface Coating and Technology, J. Am. Ceram. Soc., Metall. Mater. Trans. A, and CALPHAD. He obtained 12 invention patents (including 1 U.S. patent). In June 2023, his monograph “Computational design of engineering materials: fundamentals and case studies” was published by Cambridge University Press and promoted globally by American Society for Materials. He was selected to be National Outstanding Youth of National Natural Science Foundation of China, Cheung Kong Chair Professorship of Ministry of Education of China, Leader of Innovative Research Team of National Natural Science Foundation of China, and Leader of 973 National Basic Research Program of China. He has been awarded one First Class Prize of Hunan Provincial Natural Science, one Third Class Prize of National Natural Science of China, and one best paper prize of APDIC (Alloy Phase Diagram International Committee). Currently, he is associate Editor of CALPHAD, associate Editor of Journal of Phase Equilibria and Diffusion, associate Editor of J. Mater. Informatics, Advisory Board of International Journal of Materials Research (formerly Z. Metallkd.), and Editorial member for Vacuum, Inter. J. Mining and Metallurgy and Acta Metall. Sinica.

About the author

Yi Kong is an associate professor and doctoral supervisor at the Powder Metallurgy Research Institute of Central South University (CSU) of China. He obtained his PhD in Materials Science and Engineering from Tsinghua University in July 2007. And he spent two years as a postdoc at the University of Sydney in Australia during 2010-2012. His research mainly focuses on multi-scale computational simulations of structure-property correlation in light alloys, hard-coating, and nuclear materials. He presided over one general project and one youth fund of the National Natural Science Foundation of China, as well as one sub-task of the National Key Research and Development Program. Also, he participated as a key member in several projects such as the key project of the National Natural Science Foundation of China, the Sino-German Joint Laboratory for Microstructure of Aluminum Alloys, and the “973” Program. More than 90 SCI-indexed papers have been published or co-published in international journals such as Acta Mater., Scripta Mater., J. Alloys Compd., Appl. Surf. Sci., and MSEA, et al..

About the author

Meichen Pan now is a Master’s student under the supervision of Prof. Yong Du at Central South University (CSU) of China, and is a member of the State Key Laboratory of Powder Metallurgy. Her research focuses on finite element simulation of gradient materials. She has published 3 academic papers in J. Mater. Sci., and Materials well-known international journals.

About the author

Xiaoyu Zheng is a Ph.D. graduate from the school of the State Key Laboratory of Powder Metallurgy at Central South University, under the guidance of Prof. Yong Du. His main research focus is on crystal plasticity finite element method, with research subjects including age-hardened aluminum alloys, cemented carbides, and steel materials. He has published more than 10 academic papers in Constr. Build. Mater., J. Mater. Sci., and Materials well-known international journals.

Reference

Meichen Pan, Li Yang, Xiaoyu Zheng, Hong Mao, Yi Kong & Yong Du. Numerical simulation of fatigue fracture in gradient high-strength steel: effects of carbides and gradient structure on stress–strain response and crack propagation behavior. J Mater Sci 59, 12757–12780 (2024). https://doi.org/10.1007/s10853-024-09907-8

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