Thermal stability and phase transformation of TiO2 nanowires at various temperatures

Microelectronic Engineering, Volume 108, August 2013, Pages 134-137.
M.N. Asiah, M.H. Mamat, Z. Khusaimi, M.F. Achoi, S. Abdullah, M. Rusop

 

 

NANO-SciTech Centre, Institute of Science, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia and

Faculty of Applied Sciences, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia and

NANO-ElecTronic Centre, Faculty of Electrical Engineering, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia.

 

 

 

Abstract

 

In this paper, we report the successful synthesis of titanium dioxide nanowires by a hydrothermal method. The precursor, TiO2 nanopowder, was treated in a 10 M sodium hydroxide aqueous solution at 150 °C for 6 h, followed by annealing at 400–900 °C. The morphology and structural properties of the nanowires were investigated. The field-emission scanning electron microscopy (FESEM) images and the X-ray diffraction (XRD) pattern showed that the nanowires transformed into an anatase structure at 500 °C and that the morphology of the nanowires was maintained. At 900 °C, the nanowires transformed into a rod-like shapes with a rutile structure.

 

 

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